Cis Reports Samples For Students

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Stoichiometric Data (For any reactants that are part of the balanced equation, base on the amounts measured in lab)
Figure 3-sulfolene
Figure IR spectrum for cis-4-Cyclopentant – 1,2 dicarboxylic acid anhydride
Figure from experiment in the text

NMR 1 from lab results endo norbornene-cis-5,6 dicarboxylic anhydride

Figure 2 from lab results the exo norbornene-cis-5,6 dicarboxylic anhydride (less stable)
Theoretical from http://www.ch.ic.ac.uk/local/organic/pericyclic/p1_sigma.html

Discussion

Figure 1.The diene (1,3 butadiene) plus the ethane (sulfolene) produce a cyclohexene (either the endo or exo isomer depending on reaction conditions).
Figure 2. Under acidic conditions to sulfuric acid the endo isomer plus water form the less stable exo isomer
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Abstract

In this experiment, 5 mL of toluene solution was transferred in a 25 mL round bottom flask and then 0.40 g maleic anhydride and 0.4 g E, E-2, 4-hexadien-1-l added. Ethyl acetate was used as a solvent to carry out a TLC analysis on the mixture produced after reaction completion mainly to determine the presence of any starting material in the mixture. The reaction mixture was then slowly cooled to room temperature. There was crystallization taking place as the reaction cooled, white crystals were formed.
The mixture was further cooled in for 10 minutes in a water bath to promote crystallization to ...

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