EVALUATION OF “Ru(0) AND Ru(II) NITROSYL PINCER COMPLEXES: STRUCTURE, REACTIVITY, AND CATALYTIC ACTIVITY,” BY FOGLER ET. AL. 1) Characterization of the compound Complex 8 which is described as a Ruthenium complex with a bent nitrosyl ligand was characterized using three analytical techniques: Hydrogen NMR (1{H} NMR), X-ray Diffraction (DFT), and Infrared Spectroscopy (IR). The 1H NMR was used to verify the complex which gave a singlet signal at 56.6ppm, and its phosphine methylene ligand gave a signal at 3.27 ppm, these signals not only verify the presence of the types of hydrogen in the complex but also its ...
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Introduction
One of the classes of chemical complexes whose coordination chemistry has generated a lot of interest is the bidentate phosphines. This can be attributed to the fact that this class of ligands facilitates the combination of phosphorus atoms that have strong metal bonds with atoms from donor groups that are more labile in nature. Examples include Nitrogen atom from the aminophosphines donor group or an Oxygen atom from etherphosphines. This is unlike hard donors that are weak and basic like MeOH and H2O that do not have good binding with transitional metals including Rhenium. Due to this fact, complexes formed from ...